DISCLAIMER :

 

This section only summarizes the theoretical path of synthesis (without details/detailed instructions of the requirment for a successful reaction run. Experimental detailed details are omitted due to safety concern and legal reasons ) of some certain compounds which are subject to research and development and educational purpose only for individuals and government authoritys. Lets make any field knowladgebase available to all. (Hidding any knowladge in any field from others may strongly be related to paranoid delusional disorder of individual ( for which he already realise that its stands on fragile foundations ) again and again related to mAChRs issues with consequently cognitive decline. ) Any unskilled attempt ( from a safe or technological point of view ) to synthesize any compounds in this theoretical compound thread without prior calculation and consideration of the reaction conditions or safety precautions can lead to explosion, fire, death , permanent or temporary CNS damage , paralysis or other physical damage to themselves and others in the surroundings area, and most of them are hazardous to the environment. 

 

 

 

27.04.2025 20:44

intermediates needed :

Pyridine-2-carbaldehyde +  Ethyl (triphenylphosphanylidene)acetate = Ethyl (E)-3-(2-pyridyl)acrylate + hydrolysis esters = (E)-3-(2-Pyridyl)acrylic acid + SOLARIUM SUNBED (280-365nm) = (1R,2R,3S,4S)-2,4-Bis(2-pyridyl)-1,3-cyclobutanedicarboxylic acid + hydroxylamine HCl + base for OXIME + CH3Cl for quaternary ammonium chloride salts.

 

 

27.04.2025 18:32

general intermediates required :

Alpha-Truxillic acid , Weinreb amide formation , Grignard alkylation CH3MgBr, (R)-(+)-tert-Butylsulfinamide , (S)-(-)-tert-Butylsulfinamide , NaBH(OAc)3 , CH3I , HCl , bases , solvents.

27.04.2025 18:13

Intermediate building block required :

Alpha Truxillic acid, DPPA, CDI, NaNO2, bases, dimethylamine , 1,4-dibromobutane or Succinaldehyde , NaBH(OAc)3 , dimethyl sulfate

 

27.04.2025 15:49

Nearly 100% natural compound :

Intermediates required : Alpha-Truxillic acid , (Choline Chloride + ZnCl2 )(DES) , Solvents or coupling reagents : CDI , DCC , pyBOP...

GREEN Synthesis Directly from R'COOH (no halogenation required priorly)  w/  :

 

1. Deep Eutectic Solvents (DES)

or

2. Coupling Reaction (EDC.HCl or CDI pyBOP...)

Isomerlab d.o.o.

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 Phone: +386 40 764 332

 Email: info@isomerlab.com

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